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A two‐step reaction sequence for accessing meso‐(dialkoxyphosphoryl)porphyrins from readily available trans‐A2‐type porphyrins was developed. This approach involves bromination and subsequent palladium‐catalyzed phosphonylation. Optimal conditions for both steps were identified after exploration of various reaction parameters such as solvent, temperature and catalyst. A series of dialkoxyphosphoryl‐substituted...
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