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One-electron oxidation of the oximes R2P(=O)C(=NOH)X (X = Cl or Br) generates the nitrile oxides R2P(=O)C+=NO−, which serve as spin traps for unstable carbon-centered radicals.The latter are generated upon addition of PbO2 to a mixture of formohydroximoyl halide with an alcohol or an ether of the general formula R1OCHR2R3 under the action of atomic chlorine (bromine) released during the generation...
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