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The development of polyamide fibers with excellent mechanical performance is always a hot research topic. In this paper, the structure evolution of polyamide 1212 (PA1212) after stretching at different temperatures was characterized by Wide-Angle X-ray Diffraction (WAXD) and Small-Angle X-ray Scattering (SAXS) techniques. Experimentally, it was found that there existed a maximum tensile strength of...
Poly(hexamethylene succinate-co-hexamethylene fumarate)s (PHSF) with low hexamethylene fumarate content (CHF, between 0 and 18 mol%) were prepared and employed to explore the effect of intersegmental interaction in crystalline lattice on the polymorphism phenomenon. Wide angle X-ray diffraction (WAXD), differential scanning calorimetry (DSC) and Fourier transform infrared spectroscopy (FTIR) results...
A series of random poly(hexamethylene succinate-co-hexamethylene fumarate) (PHSF) samples was synthesized through a two-step reaction process, and their properties were systematically studied using wide angle X-ray diffraction (WAXD), differential scanning calorimetry (DSC), and Fourier transform infrared spectroscopy (FTIR). The crystal modification of polyester changes from monoclinic to orthorhombic...
Stretch-induced structural changes of poly(butylene adipate) at various temperatures were systematically investigated by X-ray diffraction method. It was found that tensile deformation could lead to both occurrence of α to β and β to α crystal transition via solid–solid process. Experimental results shows that either α or β form can be adopted as the stable phase for PBA crystal depending on the competition...
Inclusion complexes formed from host small molecules and guest polymers have provided a novel platform to study both the physical properties of isolated polymer chains and crystallization behavior of host molecules. In this report, we have studied the crystalline structure, melting behavior and infrared information of inclusion complexes formed between polyethylene glycol oligomers and urea molecules...
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