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This work reports the first synthesis of uniformly deuterated n‐dodecyl‐β‐d‐maltoside (d39‐DDM). DDM is a mild non‐ionic detergent often used in the extraction and purification of membrane proteins and for solubilizing them in experimental studies of their structure, dynamics and binding of ligands. We required d39‐DDM for solubilizing large α‐helical membrane proteins in samples for [15N–1H]TROSY...
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