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Highly crystalline spinel LiMn 2 O 4 was successfully synthesized by annealing lithiated MnO 2 at a relative low temperature of 600°C, in which the lithiated MnO 2 was prepared by chemical lithiation of the electrolytic manganese dioxide (EMD) and LiI. The LiI/MnO 2 ratio and the annealing temperature were optimized to obtain the pure phase LiMn 2 O...
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