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We report a novel NO donor (RpNO), containing a 2,6‐dimethylnitrobenzene moiety for photocontrollable NO release and a rhodamine moiety for targeting to mitochondria. Photorelease of NO from RpNO in aqueous solution was confirmed by means of ESR analysis. Cellular release of NO from RpNO was confirmed with the aid of DAF‐FM DA, an NO‐specific fluorescence probe. RpNO was colocalized with MitoTracker...
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