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Di‐tert‐butylneopentylphosphine (DTBNpP) and palladium(II) acetate provide an efficient catalytic system for the α‐arylation of ketones. Aryl bromides were coupled with ketones using 0.25–0.5 mol‐% Pd(OAc)2/DTBNpP in toluene at 50 °C, whereas aryl chlorides required a higher catalyst loading (0.5–2.0 mol‐%) and a higher temperature (80 °C). Coupling of 2‐bromophenol with ketones using the Pd/DTBNpP...
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