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The influence of water on the catalysis of biphasic Heck alkynylation, a family of palladium‐catalyzed carbon‐carbon bond formations, was investigated. Kinetic theory derived from Hatta moduli and pseudo‐stationary‐state approximations discovered that water, in coordination, reductive elimination, and product dissociation reaction steps of the deprotonation catalytic cycle, increases Gibbs energy...
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