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Hydrothermal methods were exploited in the preparation of bimetallic organic–inorganic hybrid materials of the metal-bisterpy/vanadate class. [Cu 2 (bisterpy)V 4 O 12 ]·2H 2 O exhibits a two-dimensional structure constructed from {Cu 2 V 4 O 12 } n chains linked through bisterpy ligands. The isomorphous materials [M 2 (bisterpy)V...
Hydrothermal reactions of V 2 O 5 , tetra-2-pyridylpyrazine (tpyprz) and an appropriate M(II) starting material yield a series of oxides of general composition [{M x (tpyprz)} y V 4 O 12 ] [x=1, y=2, M=Co(II), Ni(II); x=2, y=2, M=Cu(I); x=2, y=1, M=Zn(II)]. The Co(II) and Ni(II) analogues (1 and 2) are isostructural and consist of one-dimensional...
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