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The hydrolysis of uranyl‐, Nd‐ and Ce‐cations, induced by thermal decomposition of urea was investigated and the impact of the urea content and the experiment temperature on the reaction kinetics was evaluated. Uranyl precipitated as ammonium diuranate (ADU) with varying stoichiometry. Nd(III) and Ce(III) showed comparable pH evolutions and lanthanide carbonate hydroxide (LnCO3OH) products were identified,...
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