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In this work, we report the anodic electropolymerization of 4-nitro-1,2-phenylenediamine (4NoPD) in different supporting electrolytes at different pH. The feasibilities of forming the polymer poly(4-nitro-1,2-phenylenediamine) (P4NoPD) on gold and glassy carbon electrodes (GCE) were shown. The P4NoPD films were generated by continuous potential cycling between −0.15V and +1.10V (versus Ag|AgCl, saturated...
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