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The pyrochlore solid solution (Na0.33Ce0.67)2(Ir1−xRux)2O7 (0≤x≤1), containing B‐site RuIV and IrIV is prepared by hydrothermal synthesis and used as a catalyst layer for electrochemical oxygen evolution from water at pH<7. The materials have atomically mixed Ru and Ir and their nanocrystalline form allows effective fabrication of electrode coatings with improved charge densities over a typical...
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