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In water, metallic palladium on carbon was found to catalyze the deep oxidation of organophosphorus and organosulfur compounds by dioxygen at 90°C in the presence of carbon monoxide. This system presents the first examples of catalytic cleavage of phosphorus-carbon bonds. Starting with trimethylphosphine oxide, the phosphorus-containing products formed by sequential P-C cleavage were dimethylphosphinic...
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