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Nanocolloids of the intermetallic β‐CoAl phase were prepared by a soft organometallic route. They were fully characterized by (HR)TEM, EDX, WAXS, XAS and SQUID magnetometry. Their exposure to air led to an increased saturation magnetization in agreement with Co/Al segregation and the formation of Co/Al2O3 nanocomposite. Furthermore, the β‐CoAl nanoparticles could be used as seeds to grow an aluminum...
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