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Dy3+/Yb3+ co-doped Gd2O3 monodispersed nanocrystals have been synthesized using the sodium dodecyl benzene sulfonate (SDBS) as the surfactant. The SDBS surfactant plays a critical role in the forming of monodisperse Gd2O3 structures with sphere-like morphologies. The growth mechanism of the nanocrystals was proposed in detail. The samples annealed at 400 °C for 4 h exhibit good crystallinity and narrow...
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