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Two isomeric tridecafluoridotetrabromate(III) anions, [Br4F13]–, both previously predicted by quantum‐chemical calculations, have serendipitously been obtained from the reaction of BrF3 with BaF2. Single crystals of Ba2[Br3F10]2[Br4F13]2 were selected from the reaction mixture at approximately 10 °C. The crystal structure contains two novel, isomeric [Br4F13]– anions besides the known, star‐shaped...
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