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Stille-type carbonylative cross-couplings, employing palladium catalysis and Mo(CO) 6 as the carbon monoxide carrier, were used for the preparation of deoxybenzoins. Straightforward transformations were conveniently performed in closed vessels at 100°C, providing the products in good yields. Benzyl bromides and chlorides were used as coupling partners with aryl and heteroaryl stannanes. This...
Palladium catalysis was used in Stille-type carbonylative cross-couplings employing Mo(CO) 6 as the carbon monoxide source. Robust and convenient transformations were carried out in closed vessels at 100°C, providing a set of diaryl ketones in good yields. Aryl triflates and bromides were used as coupling partners with aryl stannanes. Inclusion of the Mo(CO) 6 destabilizing agent DBU...
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