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We report here spark plasma sintering (SPS) of the nonstoichiometric ultrafine-grained TiC x with the simultaneous formation of ordered carbon vacancies. The SPS-sintered TiC x exhibits interesting laminar microstructure with grains of ∼250nm in average size. The cubic superstructure of the ordered vacancies in the C sublattice is found to exist in nano domains. With the increase of...
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