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Molecular mobility and physical form of co-spray-dried sugar–lysozyme formulations were evaluated. Co-spray-dried trehalose:lysozyme and sucrose:lysozyme formulations in 1:9, 1:1 and 9:1 ratios (w:w) were stored at 0% RH and 75% RH for 5–6 days. Molecular mobility and physical form of the co-spray-dried formulations after storage were determined by using 13 C and 1 H solid-state NMR...
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