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A starburst-shaped ligand, 4,4′4″-tris[N,N-bis(2-pyridylmethyl) aminomethyl] triphenylamine, and its palladium and copper trinuclear complexes were designed and prepared. NMR techniques, COSY and ROESY, were applied to the palladium complex to examine its conformation in solution. The palladium complex was found to prefer a folded conformation even at 75°C, indicating the occurrence of strong intramolecular...
A ligand, 4-methoxy-4′,4″-bis[N,N-bis(2-pyridylmethyl) aminomethyl]triphenyl-amine, and its palladium and copper dinuclear complexes were designed and prepared in order to examine intramolecular interactions between an organic cation radical and the metal ion. Novel NMR techniques, COSY and NOESY, were applied to the palladium complex to examine its conformation in solution. The palladium complex...
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