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A novel discrete neutral Cd17 sulfide cluster (denoted CMM‐9) with seven corners has been synthesized by slow diffusion of methanol into a mixed solution (DMF/CS2 = 1:1, weight ratio) containing an ionic starting material CMM‐4. The structures of CMM‐4 and CMM‐9 are determined from single crystal X‐ray diffraction data collected at 150 K. The structure of the new Cd17 cluster is distinctly different...
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