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The thermal reaction of the tetranuclear cluster HIrRu 3 (CO) 13 with ethylene in hexane (90 o C, 2 bar) affords, in addition to H 3 IrRu 3 (CO) 12 , the pentanuclear cluster HIrRu 4 (CO) 15 (μ 4 -C-CH 3 ) (1) in which the ethylidyne ligand is coordinated through a carbon atom to the four ruthenium atoms...
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