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The admixture of CeO2, Ce, CeCl3, and MoO3 with an excess of LiCl as flux in evacuated silica ampules leads to large black single crystals as well as a black microcrystalline powder of Ce3Cl3[MoO6] after tempering at 850 °C for three days. The title compound crystallizes in the hexagonal space group P63/m (a=934.93(4), c=538.86(2) pm) with two formula units per unit cell. The crystal structure consists...
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