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The [(TPA)FeIII(TCC)]+ complex [TPA = tris(2‐pyridylmethyl)amine, TCC2– = 3,4,5,6‐tetrachlorocatecholate dianion] forms a molecular solid with the SbF6– anion, which exhibits an incomplete S = 1/2 ↔ S = 5/2 thermal spin‐crossover process centered at 250 K. Single‐crystal X‐ray diffraction, Raman spectroscopy, and magnetic measurements of this orthorhombic polymorph were performed to delineate the...
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