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Nanostructures of FeSex with a tetragonal PbO‐type phase have been grown through a new and simple solvothermal route. By adding polyvinyl pyrrolidone (PVP) as a controlling reagent, the products change from nanoflowers to regular square nanoplates. Both the phase and structure are identified by powder X‐ray diffraction and electron microscopy. The square nanoplates are revealed to be enclosed by two...
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