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A new porous 2D metal–organic framework [Cu(L)DMF]·2H 2 O (1) has been synthesized by self-assembling copper paddle-wheel units with an asymmetrical dicarboxylate ligand prolonged by alkyne groups, 3,3′-(ethyne-1,2-diyl)dibenzoic acid (H 2 L) under solvothermal condition. The activated sample 1a displays selective adsorption of CO 2 over N 2 and shows low isosteric...
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