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Zn,Al-layered double hydroxides (LDHs) intercalated by an anionic oxomolybdenum guest were prepared by ion-exchange of precursor Zn,Al-NO 3 LDHs with the complex [NMe 4 ] 2 [MoO 2 (3,4-dhb) 2 ] (3,4-H 2 dhb=3,4-dihydroxybenzoic acid). Powder X-ray diffraction (XRD) showed that the basal spacing increased from 8.7 to 8.9Å for the precursor materials to...
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