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Procedures are described for the synthesis of tetranuclear manganese carboxylate complexes with ligands derived from 4-imidazoleacetic acid (imidacH) and 4-imidazolecarboxylic acid (imidcarbH). Reaction mixtures containing NBu n4 imidac or NHex n4 imidcarb generated in situ and either [Mn 3 O(O 2 CMe) 6 (py) 3 ](ClO 4 ) or Mn(O ...
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