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The N 4 O 3 coordinating heptadentate imidazolidinyl phenolate ligand, H 3 L (2-(2′-hydroxyphenyl)-1,3-bis[4-(2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine) forms with Cu(II) a rare aqua bridged complex [{Cu 2 (μ-L)(μ-H 2 O)} 2 ](ClO 4 ) 2 ·4.5H 2 O (1·4.5H 2 O). Complex 1·4.5H 2 O contains two crystallographically...
Atmospheric CO 2 fixation in basic medium (initial pH 8.5) leads to a novel hydrogencarbonate single-oxygen bridged dicopper(II) complex [Cu2II(L)(HCO3)]·4H2O(1·4H2O) from the dinucleating ligand H 3 L (2-methyl-2-(2′-hydroxyphenyl)-1,3-bis[4-methyl-4-(2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine). The same reaction in neutral medium (initial pH 6) gives the monocopper(II) complex...
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