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The nucleophilic attack of an IrIII isocyanide complex bearing a tetradentate pyridine‐carboxamide ligand with amines to give carbene and carbamoyl complexes has been studied. The treatment of Na[Ir(bpb)Cl2] {bpb2– = dianion of 1,2‐bis(2‐pyridinecarboxamido)benzene} with PR3 (R = p‐tolyl) in refluxing glycol gave [Ir(bpb)(PR3)Cl] (1). Chloride abstraction of 1 with silver tosylate (AgOTs) led to isolation...
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