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Zr(NR2)2[MeC(NiPr)2]2 (R=Me, 1; Et, 2) have been prepared through aminolysis and their reactions with O2 and water have been studied. Two major products from the reactions are the oxo dimer {(μ-O)Zr[MeC(NiPr)2]2}2 (3) and its insoluble polymer {(μ-O)Zr[MeC(NiPr)2]2}n (4). Over time the dimer 3 polymerizes to 4. Zr peroxo trimer {(μ-η2:η2-O2)Zr[MeC(NiPr)2]2}3 (5) was also observed from the reaction...
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