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The paramagnetic triple‐decker complexes [(Cp*Ru)2{μ‐(CMe)3(BCl)(BMe)}] (3b) and [(Cp*Ru)2{μ‐(CMe)3(BCl)2}] (3c) are formed by refluxing a mixture of [Cp*RuCl]4 and pentamethyl‐2,3‐dihydro‐1,3‐diborole in thf. In CH2Cl2 under air complex 3b slowly looses a hydrogen atom with formation of the diamagnetic triple‐decker [(Cp*Ru)2{μ‐η5:η6‐(CMe)3(BCl)(BCH2)}] (4b) with the unsymmetrical dihydrodiborafulvene...
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