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A palladium(II) complex of our π-expanded ligand, i.e., a salicylaldimine-style ligand based on pyrene, was synthesized and characterized. A treatment of this ligand (L) with palladium(II) acetate afforded the desired metal complex, Pd(II)L2, 3(Pd). Single crystal diffraction study revealed that this complex is a square planar four-coordinate palladium(II) complex. The structure of 3(Pd), i.e., shapes...
A pyrene-based new ligand (1) attaching hydroxyl and imine group, i.e., a salicylaldimine-style ligand based on pyrene, was designed and synthesized. The ligand was prepared from the commercially available pyrene in five steps. A treatment of this ligand 1 (L) with Pt(II)Cl2(PhCN)2 in the presence of AcONa in PhCl afforded the corresponding metal complex, Pt(II)L2 (2) (80%). Single crystal diffraction...
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