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Die elektrokatalytische H2‐Erzeugung durch einen molekularen Katalysator mit einem billigen Metall kann zur Lösung von Umweltproblemen beitragen. H. Masuda et al. beschreiben in der Zuschrift auf S. 5333 ff. die Synthese eines NiII‐Komplexes mit einem zweizähnigen Phosphanylpyridylliganden und einer Aminbase als Protonentransferzentrum, der die H2‐Bildung katalysiert. Elektrochemische Messungen ergaben,...
A novel nickel(II) complex [Ni(L)2Cl]Cl with a bidentate phosphinopyridyl ligand 6‐((diphenylphosphino)methyl)pyridin‐2‐amine (L) was synthesized as a metal‐complex catalyst for hydrogen production from protons. The ligand can stabilize a low Ni oxidation state and has an amine base as a proton transfer site. The X‐ray structure analysis revealed a distorted square‐pyramidal NiII complex with two...
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