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Zn/Al-LDHs with cationic ratio of 1–4 were prepared by the co-precipitation method at constant pH. The XRD patterns showed that additional phase is present in all samples due to the lattice strains created when more Zn 2+ is added and the longer periods of hydrothermal treatment. The as-synthesized samples were calcined at different temperatures and the phase transformations were fully investigated...
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