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The crystal structures of synthetic 1-galactosamide bolaamphiphiles, N,N'-bis(β-d-galactopyranosyl)decane-1,10-dicarboxamide (1) and N,N'-bis(β-d-galactopyranosyl)dodecane-1,12-dicarboxamide (2), were determined by single-crystal X-ray analysis. The space groups are P2 1 , Z=2 with cell dimensions: a=13.624(2), b=4.832(3), c=21.178(3) 9, β=98.57(1) o for 1; a=13.521(2), b=4.838(1),...
The crystal structure of the synthetic 1-glucosamide bolaamphiphile N,N -bis(β-d-glucopyranosyl)undecane-1,11-dicarboxamide (1) was determined by single-crystal X-ray analysis. The space group is P2 1 with cell dimensions: a = 6.220(1), b = 48.25(1), c = 4.922(2) 9, β = 105.67(2)°, and Z = 2. The glucopyranosyl ring is in a 4 C 1 chair conformation. The bolaamphiphile...
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