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This study reports the synthesis of three types of aluminium (Al)‐modified polyborosilazane ceramic precursors (PBSAZ) from C8H19Al/HSiCl3/HMDZ/BCl3 and their thermal conversion to SiBNC‐Al ceramics at 1000°C. FT‐IR, nuclear magnetic resonance (NMR), X‐ray photoelectron spectroscopy (XPS), and thermogravimetric analysis (TGA) are used to characterize the structures and properties of the PBSAZ. PBSAZ...
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