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The synthesis and characterization of a cobaltocenium-based redox-active cryptand 3 containing a phenanthroline unit is described. Complex formation (with Ca 2+ ) was studied by 1 H/ 13 C-NMR, and the effects of complexation on the redox properties of 3 were monitored by cyclic voltammetry. The fluorescence spectra of the complexes of 3 and its ferrocene analogue...
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