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The Huisgen thermal reaction between an organic azide and an acetylene was employed for the selective monofunctionalization of a X6‐azacryptand ligand bearing a tren coordinating unit [X6 stands for calix[6]arene and tren for tris(2‐aminoethyl)amine]. Supramolecular assistance, originating from the formation of a host–guest inclusion complex between the reactants, greatly accelerates the reaction...
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