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A small library of structurally diverse primary amines bearing a geminal CF 3 group was synthesized on a preparative scale. The synthesis starts with an aldehyde or ketone that reacts with benzylamine yielding the corresponding imine. The latter is then trifluoromethylated with Me 3 SiCF 3 under acidic conditions to give a benzylalkylamine. In the last step the Pd-mediated...
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