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A series of cobalt complexes with pentadentate pyridine‐rich ligands is studied. An initial CoII amine complex 1 is prone to aerial oxidation yielding a CoIII imine complex 2 that is further converted into an amide complex 4 in presence of adventitious water. Introduction of an N‐methyl protecting group to the ligand inhibits this oxidation and gives rise to the CoII species 5. Both the CoIII4 and...
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