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An efficient method was described for the synthesis of nano-sized flake carboxymethyl cassava starch (CMCS) with high-degree substitution under ultrasonic irradiation. The scanning electron micrographs (SEM) revealed that nano-sized CMCS flakes with the substitution degree of 1.15 were in shape of hexagon with smooth surface and with the size of 100–400nm. The substitution degree of carboxymethylation...
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