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The hydroalkoxycarbonylation of terminal arylacetylenes can be carried out in an easy one-step synthesis through the use of PdI 2 or PdI 2 /KI as catalytic systems under non-oxidative conditions, without other ligands and in the absence of added acids. Going from non-polar to polar reaction media, we have noticed a dramatic change in the chemoselectivity of the reaction with prevailing...
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