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A series of 13C‐labeled polyaromatic hydrocarbons (PAHs), fluorenols and phenanthrenols were synthesized from commercially available 13C‐labeled starting material giving rise to M + 6 isotopomers. This was accomplished using key palladium‐catalyzed cross‐coupling and one‐carbon homologation strategies. The conditions for these reactions were optimized, and the new chemical routes are efficient in...
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