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Composition depth profiles of d.c.-plated and pulse-plated Fe–Ni alloys have been investigated with the reverse depth profile analysis method. When d.c. plating is applied, the mole fraction of iron near the substrate is higher than during steady-state deposition since iron is preferentially deposited beside nickel and the achievement of the steady-state deposition condition takes time. The steady-state...
Depth profile of electrodeposited Fe–Co–Ni alloys was measured using secondary neutral mass spectrometry with the reverse sputtering direction. A spontaneous near-substrate composition modulation was found for each sample studied. The initial deposit is very rich in Fe, which decays due to the depletion of the electrolyte in the vicinity of the cathode surface. The near-substrate modulation pattern...
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