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Sensitive SIFTing: Multidimensional non‐uniform sampling (NUS) NMR spectroscopy is extended to the severely sensitivity‐limited regime typical of MAS NMR of biomacromolecules by the use of spectroscopy by the integration of frequency and time domain information (SIFT). A three‐dimensional MAS NMR experiment is expedited (here 3.4‐fold) without losing sensitivity or resolution.
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