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Three tetranuclear heterometallic ZnII‐LnIII complexes of the 30‐membered [3+3] hexaimine macrocycle (LEt)6–, with general formula ZnII3LnIII(LEt)(NO3)2OAc·5H2O (LnIII = DyIII, ErIII, YbIII), were prepared using our established one‐pot synthesis methodology, whereby the individual components of the whole system are poised to assemble themselves into a mixed 3d/f4f macrocyclic system. This uses a 3:1:3:3...
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