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A Fe3+ complex with N3S3‐type tripod ligand, 1, reacts with O2 in CH3OH to generate formaldehyde, which has been studied structurally, spectroscopically, and electrochemically. Complex 1 crystallizes as an octahedral structure with crystallographic C3 symmetry around the metal, with Fe‐N=2.2917(17) Å and Fe‐S=2.3574(6) Å. UV‐vis spectrum of 1 in CH3OH under Ar shows an intense band at 572 nm (ϵ 4,100...
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