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The preparation and properties of [M(chelate)X 2 ] complexes are reported, where M=Co(II) or Ni(II), chelate=2,5-diphenyl-3,4-bis(2-pyridyl)cyclopentadienone and X=Cl or Br. These complexes have been characterized by elemental analyses and spectroscopic methods. The crystal and molecular structures of CoLCl 2 ·0.5CH 3 CN (1) and NiLBr 2 ·CHCl 3 (4) have been...
Reaction of nickel(II) ions with diisopropylaminoethanethiolate ligands has been found to be self-assembled in the solution to obtain an unexpected pentanuclear cluster of the title compound. Characterization of the product by single-crystal X-ray crystallography revealed that it consists of a homoleptic nickel thiolate with a pentagonal-prismatic sulfur framework. An efficient method of the data...
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