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Unsupported Co promoted MoS2 catalysts for the hydrodesulfurization (HDS) reaction were prepared using a mixture of Co(dien)2MoS4 (dien = diethylenetriamine) and tetrapropylammonium thiomolybdate. The mixture was first treated in a high energy ball mill followed either by ex situ activation in forming gas or by in situ activation during the HDS reaction. The ex situ activation mode leads to a very...
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